Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL13C1 |
Synchrotron site | NSRRC |
Beamline | BL13C1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-12-03 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.99 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 113.931, 113.931, 144.357 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 98.670 - 2.740 |
R-factor | 0.20303 |
Rwork | 0.201 |
R-free | 0.24617 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | TEAD4 in 3JUA |
RMSD bond length | 0.015 |
RMSD bond angle | 1.854 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0189) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 98.670 | 2.810 |
High resolution limit [Å] | 2.740 | 2.740 |
Rmerge | 0.059 | 0.580 |
Number of reflections | 28983 | 1974 |
<I/σ(I)> | 2.7 | |
Completeness [%] | 99.7 | 98.87 |
Redundancy | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.9 | 298 | 1M phosphate buffer |