5YZZ
AtVAL1 B3 domain in complex with 13bp-DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-11-30 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97853 |
Spacegroup name | I 41 2 2 |
Unit cell lengths | 86.896, 86.896, 148.237 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.580 |
R-factor | 0.22757 |
Rwork | 0.226 |
R-free | 0.25522 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5yzy |
RMSD bond length | 0.013 |
RMSD bond angle | 1.895 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0189) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 74.970 | 2.670 |
High resolution limit [Å] | 2.580 | 2.580 |
Rmerge | 0.077 | |
Number of reflections | 9191 | |
<I/σ(I)> | 29.4 | |
Completeness [%] | 99.5 | |
Redundancy | 13.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 30% (w/v) PEG 5000 MME, 0.1M Tris base/Hydrochloric acid pH 8.0, 0.2M Lithium sulfate |