5YY7

Crystal structure of Arabidopsis thaliana HPPD complexed with Benquitrione

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-03-10
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	0.97780
Spacegroup name	P 41 21 2
Unit cell lengths	94.928, 94.928, 185.031
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	47.464 - 3.298
R-factor	0.2732
Rwork	0.271
R-free	0.30600
RMSD bond length	0.002
RMSD bond angle	0.414
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	3.416
High resolution limit [Å]	3.298	3.298
Number of reflections	13347
<I/σ(I)>	6.4
Completeness [%]	100.0
Redundancy	6.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291.16	PEG 400, sodium chloride, Sodium acetate