5YUG

AtVAL1 PHD-Like domain in the P31 space group

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-11-17
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	0.97737
Spacegroup name	P 31
Unit cell lengths	52.228, 52.228, 121.674
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	26.114 - 1.570
R-factor	0.222
Rwork	0.220
R-free	0.25440
Structure solution method	SAD
RMSD bond length	0.006
RMSD bond angle	0.915
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	SHELXCD
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.630
High resolution limit [Å]	1.570	1.570
Rmerge	0.142
Number of reflections	51823
<I/σ(I)>	16
Completeness [%]	99.8
Redundancy	10.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	0.2M Ammonium citrate tribasic pH 7.0, 20% w/v Polyethylene glycol 3350