5YSK
SdeA mART-C domain EE/AA apo
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL44XU |
| Synchrotron site | SPring-8 |
| Beamline | BL44XU |
| Temperature [K] | 193 |
| Detector technology | CCD |
| Collection date | 2017-06-19 |
| Detector | Bruker DIP-6040 |
| Wavelength(s) | 0.9 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 43.750, 85.360, 70.795 |
| Unit cell angles | 90.00, 97.11, 90.00 |
Refinement procedure
| Resolution | 32.420 - 2.403 |
| R-factor | 0.1926 |
| Rwork | 0.185 |
| R-free | 0.26140 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.213 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 32.420 |
| High resolution limit [Å] | 2.403 |
| Number of reflections | 19830 |
| <I/σ(I)> | 34.6762 |
| Completeness [%] | 98.0 |
| Redundancy | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | PEG400, Tris |
