5YR9
Crystal Structure of Cypovirus Polyhedra R13A/E73C/Y83C Mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL32XU |
Synchrotron site | SPring-8 |
Beamline | BL32XU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-10-22 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 1.0 |
Spacegroup name | I 2 3 |
Unit cell lengths | 103.750, 103.750, 103.750 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.680 - 1.700 |
R-factor | 0.16234 |
Rwork | 0.158 |
R-free | 0.20470 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.019 |
RMSD bond angle | 1.863 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 36.680 |
High resolution limit [Å] | 1.700 |
Number of reflections | 18547 |
<I/σ(I)> | 8.49 |
Completeness [%] | 100.0 |
Redundancy | 27.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | IN CELL | 300 | In vivo crystallization in the cytoplasm of the cell, temperature 300 K |