Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL40B2 |
| Synchrotron site | SPring-8 |
| Beamline | BL40B2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-11-04 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.9792, 0.9794, 0.9851 |
| Spacegroup name | H 3 2 |
| Unit cell lengths | 76.822, 76.822, 85.888 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 38.410 - 2.503 |
| R-factor | 0.2264 |
| Rwork | 0.223 |
| R-free | 0.26550 |
| Structure solution method | MAD |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.831 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 38.410 | 2.590 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Number of reflections | 3504 | 337 |
| <I/σ(I)> | 34.4 | 9.03 |
| Completeness [%] | 99.9 | 99.4 |
| Redundancy | 20.9 | 18.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7 | 293 | Ammonium Sulfate, HEPES, pH 7.0 |
