5YC1
TRAF4_GPIb complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 5C (4A) |
| Synchrotron site | PAL/PLS |
| Beamline | 5C (4A) |
| Temperature [K] | 110 |
| Detector technology | PIXEL |
| Collection date | 2016-09-22 |
| Detector | DECTRIS PILATUS 300K |
| Wavelength(s) | 1.000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 56.716, 88.594, 120.757 |
| Unit cell angles | 90.00, 93.62, 90.00 |
Refinement procedure
| Resolution | 33.781 - 2.506 |
| R-factor | 0.2141 |
| Rwork | 0.211 |
| R-free | 0.26490 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.390 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.500 |
| Number of reflections | 42567 |
| <I/σ(I)> | 21.7 |
| Completeness [%] | 95.0 |
| Redundancy | 3.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 298 | magnesium formate dehydrate, polyethylene glycol 3350 |
