5YC0
Crystal structure of LP-46/N44
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U1 |
| Synchrotron site | SSRF |
| Beamline | BL17U1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2016-03-17 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9796 |
| Spacegroup name | P 1 |
| Unit cell lengths | 34.091, 53.259, 59.344 |
| Unit cell angles | 94.42, 96.52, 90.02 |
Refinement procedure
| Resolution | 27.098 - 2.000 |
| R-factor | 0.222 |
| Rwork | 0.220 |
| R-free | 0.25630 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.436 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 27.100 |
| High resolution limit [Å] | 2.000 |
| Number of reflections | 26727 |
| <I/σ(I)> | 12.3 |
| Completeness [%] | 96.0 |
| Redundancy | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291.15 | 8%(v/v) Tacsimate pH 4.0, 20%(w/v) Polyethylene glycol 3,350 |
