5Y14
Crystal structure of LP-40/N44
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U1 |
| Synchrotron site | SSRF |
| Beamline | BL17U1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2016-06-27 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9796 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 50.830, 36.140, 53.440 |
| Unit cell angles | 90.00, 99.87, 90.00 |
Refinement procedure
| Resolution | 24.284 - 1.762 |
| R-factor | 0.2099 |
| Rwork | 0.207 |
| R-free | 0.25060 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.662 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.760 |
| Number of reflections | 17147 |
| <I/σ(I)> | 16 |
| Completeness [%] | 90.4 |
| Redundancy | 3.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291.15 | 2.2M Sodium chloride, 0.1M Tris pH 8.5 |
