5XYB

Crystal structure of AimR from Bacillus phage SPbeta

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	CCD
Collection date	2017-04-05
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.97915
Spacegroup name	P 2 21 21
Unit cell lengths	33.571, 114.814, 220.444
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	45.238 - 2.198
R-factor	0.2168
Rwork	0.214
R-free	0.27540
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	0.896
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX (1.10.1_2155)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.198
Number of reflections	44514
<I/σ(I)>	6
Completeness [%]	99.2
Redundancy	7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291.5	PEG 8000, dithiothreitol, Sodium Bromine, Sodium Cacodylate