5XU5
Complex structure of RmMan134A-M4
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL18U1 |
| Synchrotron site | SSRF |
| Beamline | BL18U1 |
| Temperature [K] | 80 |
| Detector technology | PIXEL |
| Collection date | 2016-11-22 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 0.977 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 44.696, 59.002, 104.983 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 41.100 - 2.020 |
| Rwork | 0.156 |
| R-free | 0.21490 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | HKL-3000 |
| Data scaling software | HKL-3000 |
| Phasing software | HKL-3000 |
| Refinement software | PHENIX (dev-2474-000) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 41.120 | |
| High resolution limit [Å] | 2.020 | 2.020 |
| Rmerge | 0.087 | |
| Number of reflections | 17179 | |
| <I/σ(I)> | 8.3 | |
| Completeness [%] | 92.0 | 92 |
| Redundancy | 3.5 | 3.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | Tris-Hcl, tri-Sodium Citrate |
