5XSJ
XylFII-LytSN complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-04-27 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.9798 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 105.681, 143.688, 87.133 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.182 - 2.202 |
R-factor | 0.1956 |
Rwork | 0.194 |
R-free | 0.21830 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.058 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.200 |
Number of reflections | 33221 |
<I/σ(I)> | 14.61 |
Completeness [%] | 97.9 |
Redundancy | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.6 | 293 | 0.2 M lithium sulfate, 2.0 M ammonium sulfate, 0.1 M MES pH 6.6 |