5XRH

Galectin-10/Charcot-Leyden crystal protein crystal structure

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-03-19
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.9
Spacegroup name	P 65 2 2
Unit cell lengths	48.559, 48.559, 260.328
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.497 - 1.550
R-factor	0.1732
Rwork	0.172
R-free	0.19570
Refinement software	PHENIX (1.10.1_2155)

Data quality characteristics

	Overall
Low resolution limit [Å]	19.500
High resolution limit [Å]	1.550
Number of reflections	27731
<I/σ(I)>	24.3
Completeness [%]	99.7
Redundancy	17.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	Bis-Tris