5XQZ

Structure of the MOB1-NDR2 complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	CCD
Collection date	2013-12-11
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.99999
Spacegroup name	P 21 21 21
Unit cell lengths	57.519, 94.424, 102.200
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 - 2.100
R-factor	0.16084
Rwork	0.156
R-free	0.24374
RMSD bond length	0.015
RMSD bond angle	1.550
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	REFMAC (5.6.0117)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.100
Number of reflections	32723
<I/σ(I)>	16.3
Completeness [%]	99.6
Redundancy	6.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		287	PEG 3350, HEPES, magnesium chloride