5XQH
Crystal structure of truncated human Rogdi
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 5C (4A) |
| Synchrotron site | PAL/PLS |
| Beamline | 5C (4A) |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-07-08 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.97940 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 63.364, 114.695, 44.205 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 34.570 - 2.040 |
| Rwork | 0.200 |
| R-free | 0.24700 |
| Structure solution method | SAD |
| Phasing software | PHENIX |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | |
| High resolution limit [Å] | 2.040 | 2.040 |
| Rmerge | 0.082 | 0.469 |
| Number of reflections | 39509 | |
| <I/σ(I)> | 49.8 | 5.9 |
| Completeness [%] | 99.9 | 99.9 |
| Redundancy | 9.4 | 9.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 277.15 | 11% PEG 4000, 100mM MES pH 6.5, 5mM DTT |
