5XP7

C-Src in complex with ATP-CHCl

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	80
Detector technology	CCD
Collection date	2016-12-21
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.979
Spacegroup name	P 1
Unit cell lengths	42.276, 63.978, 74.003
Unit cell angles	101.03, 89.83, 90.60

Refinement procedure

Resolution	36.551 - 2.012
R-factor	0.1692
Rwork	0.168
R-free	0.19820
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.205
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	PHENIX
Refinement software	PHENIX (1.8.4_1496)

Data quality characteristics

	Overall
Low resolution limit [Å]	36.600
High resolution limit [Å]	2.000
Number of reflections	48688
<I/σ(I)>	13.9
Completeness [%]	96.5
Redundancy	3.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	PEG4000