5XMZ

Verticillium effector PevD1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	100
Detector technology	CCD
Collection date	2012-05-01
Detector	MAR CCD 130 mm
Wavelength(s)	1.5418
Spacegroup name	C 2 2 21
Unit cell lengths	58.000, 79.489, 55.512
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	35.805 - 1.850
R-factor	0.2044
Rwork	0.202
R-free	0.26020
Structure solution method	SAD
RMSD bond length	0.007
RMSD bond angle	1.239
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX (1.8.2_1309)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.850
Rmerge	0.040
Number of reflections	11198
<I/σ(I)>	15.3
Completeness [%]	98.4
Redundancy	6.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	BATCH MODE		293	0.5M Sodium Formate, Tris pH7.5