5XI3

BRD4 bound with compound Bdi3

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	CCD
Collection date	2016-12-06
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.9792
Spacegroup name	P 21 21 21
Unit cell lengths	32.478, 47.581, 78.714
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.327 - 1.674
R-factor	0.1883
Rwork	0.187
R-free	0.21780
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.967
Data scaling software	XDS
Refinement software	PHENIX ((1.11_2567: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	30.330
High resolution limit [Å]	1.674
Number of reflections	14195
<I/σ(I)>	17.43
Completeness [%]	96.8
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	293	1.5M NAFORMATE, 5% GLYCEROL