5XG8

Galectin-13/Placental Protein 13 variant R53H crystal structure

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-03-19
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.9
Spacegroup name	C 2 2 2
Unit cell lengths	58.037, 92.207, 50.703
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.092 - 1.550
R-factor	0.1733
Rwork	0.171
R-free	0.19460
Structure solution method	MOLECULAR REPLACEMENT
Refinement software	PHENIX (1.10.1_2155: ???)

Data quality characteristics

	Overall
Low resolution limit [Å]	19.092
High resolution limit [Å]	1.550
Number of reflections	20107
<I/σ(I)>	18.3
Completeness [%]	99.5
Redundancy	6.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG