5X40
Structure of a CbiO dimer bound with AMPPCP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NFPSS BEAMLINE BL19U1 |
| Synchrotron site | NFPSS |
| Beamline | BL19U1 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2016-05-05 |
| Detector | MAR555 FLAT PANEL |
| Wavelength(s) | 0.97853 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 71.339, 74.399, 106.849 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 29.665 - 1.450 |
| R-factor | 0.1573 |
| Rwork | 0.157 |
| R-free | 0.17740 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.424 |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 1.450 |
| Number of reflections | 101455 |
| <I/σ(I)> | 23.3 |
| Completeness [%] | 99.9 |
| Redundancy | 6.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.64M sodium acetate, pH 4.6, 18% PEG 3350 |
