5X1R
PpkA-294 apo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | AREA DETECTOR |
Collection date | 2015-06-29 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97853 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 59.100, 65.500, 78.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.600 |
R-factor | 0.1867 |
Rwork | 0.185 |
R-free | 0.21630 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.065 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_2247: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.670 |
High resolution limit [Å] | 1.590 | 1.590 |
Rmerge | 0.058 | 0.403 |
Rpim | 0.017 | 0.127 |
Number of reflections | 40724 | 5206 |
<I/σ(I)> | 20.5 | 4.4 |
Completeness [%] | 98.1 | 87.8 |
Redundancy | 12.6 | 10.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 295 | PEG3350, sodium chloride |