5WXM

Crystal structure of the Imp3 and Mpp10 complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	100
Detector technology	CCD
Collection date	2013-01-01
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.97915
Spacegroup name	P 21 21 21
Unit cell lengths	51.565, 86.951, 88.720
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	33.629 - 2.304
R-factor	0.1962
Rwork	0.194
R-free	0.23720
Structure solution method	SIRAS
RMSD bond length	0.008
RMSD bond angle	0.917
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	PHENIX
Refinement software	PHENIX ((1.11rc1_2513: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.300
Number of reflections	18226
<I/σ(I)>	15.4
Completeness [%]	99.9
Redundancy	6.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	5	293	0.2 M potassium sodium tartrate, 0.1 M sodium citrate, 1.7 M ammonium sulfate