5WRR
Crystal structure of Fam20A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-01-14 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 156.854, 156.854, 143.655 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.136 - 2.506 |
R-factor | 0.2158 |
Rwork | 0.215 |
R-free | 0.23140 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4kqa |
RMSD bond length | 0.002 |
RMSD bond angle | 0.617 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.540 |
High resolution limit [Å] | 2.500 | 6.780 | 2.500 |
Rmerge | 0.172 | 0.088 | 1.804 |
Number of reflections | 70256 | ||
<I/σ(I)> | 9.4 | ||
Completeness [%] | 99.9 | 98.5 | 100 |
Redundancy | 10.9 | 9.7 | 11.1 |
CC(1/2) | 0.993 | 0.841 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 291 | ammonium sulfate, HEPES, PEG 400 |