5WRA
Crystal structure of hen egg-white lysozyme
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | FREE ELECTRON LASER |
| Source details | SACLA BEAMLINE BL3 |
| Synchrotron site | SACLA |
| Beamline | BL3 |
| Temperature [K] | 299 |
| Detector technology | CCD |
| Collection date | 2015-04-05 |
| Detector | MPCCD |
| Wavelength(s) | 0.95 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 79.600, 79.600, 38.300 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 26.075 - 1.450 |
| R-factor | 0.1813 |
| Rwork | 0.180 |
| R-free | 0.19630 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.071 |
| Data scaling software | CrystFEL |
| Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 1.450 |
| Number of reflections | 22415 |
| <I/σ(I)> | 13.4 |
| Completeness [%] | 100.0 |
| Redundancy | 945 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | BATCH MODE | 299 | sodium chloride, PEG 6000, pH 3.0 |
