5W7K
Crystal structure of OxaG
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 23-ID-D |
| Synchrotron site | APS |
| Beamline | 23-ID-D |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-10-12 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 0.979 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 121.628, 36.208, 126.304 |
| Unit cell angles | 90.00, 102.83, 90.00 |
Refinement procedure
| Resolution | 49.315 - 1.994 |
| R-factor | 0.2223 |
| Rwork | 0.220 |
| R-free | 0.25950 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.968 |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 49.315 |
| High resolution limit [Å] | 1.990 |
| Rmerge | 0.124 |
| Number of reflections | 36979 |
| <I/σ(I)> | 9.84 |
| Completeness [%] | 99.1 |
| Redundancy | 6.4 |
| CC(1/2) | 0.996 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.7 | 293 | PEG 3350, MPD, magnesium chloride, bis-tris |
