5W5P

Crystal structure of Acinetobacter baumannii phage AM24 tailspike protein

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2015-09-18
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.979
Spacegroup name	P 63 2 2
Unit cell lengths	100.657, 100.657, 307.836
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	47.836 - 2.429
R-factor	0.182
Rwork	0.180
R-free	0.21710
Structure solution method	SAD
RMSD bond length	0.003
RMSD bond angle	0.554
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	SHELXDE
Refinement software	PHENIX ((dev_2666: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.429	2.429
Number of reflections	64571
<I/σ(I)>	21.04
Completeness [%]	97.9
Redundancy	20

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	5	293.15	38% PEG1000, 120 mM magnesium sulfate, 100 mM sodium citrate