Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 5.0.2 |
| Synchrotron site | ALS |
| Beamline | 5.0.2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-05-20 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 1.00000 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 104.840, 72.373, 105.613 |
| Unit cell angles | 90.00, 96.55, 90.00 |
Refinement procedure
| Resolution | 48.920 - 2.300 |
| R-factor | 0.2178 |
| Rwork | 0.216 |
| R-free | 0.24120 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4XRV |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.888 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.920 | 2.380 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Rmerge | 0.062 | 0.450 |
| Rpim | 0.032 | 0.268 |
| Number of reflections | 34922 | 3427 |
| <I/σ(I)> | 12.2 | 2.2 |
| Completeness [%] | 99.5 | 90.3 |
| Redundancy | 3.6 | 3.7 |
| CC(1/2) | 0.998 | 0.903 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | BATCH MODE | 7 | 293 | Sodium Formate 4.0-4.5 M, Bis-tris propane 0.1 M |
