5VY1
Crystal structure of the extended Tudor domain from BmPAPI
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2015-06-26 |
Detector | RIGAKU |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 65.717, 65.717, 225.431 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.064 - 3.050 |
R-factor | 0.2554 |
Rwork | 0.253 |
R-free | 0.29600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5vqg |
RMSD bond length | 0.002 |
RMSD bond angle | 0.654 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.500 | 3.200 |
High resolution limit [Å] | 3.050 | 3.050 |
Rmerge | 0.171 | 0.572 |
Number of reflections | 8655 | 1274 |
<I/σ(I)> | 5.9 | 2.1 |
Completeness [%] | 87.9 | 90.3 |
Redundancy | 3 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 291.2 | 0.95 M ammonium sulfate, 50 mM sodium acetate, pH 5.5 and 5% glucose. |