5VLM

Crystal structure of EilR in complex with crystal violet

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.2.2
Synchrotron site	ALS
Beamline	8.2.2
Temperature [K]	100
Detector technology	AREA DETECTOR
Collection date	2014-10-14
Detector	ADSC QUANTUM 315r
Wavelength(s)	1.000
Spacegroup name	P 1 21 1
Unit cell lengths	97.397, 79.229, 105.579
Unit cell angles	90.00, 97.10, 90.00

Refinement procedure

Resolution	48.644 - 3.403
R-factor	0.2115
Rwork	0.205
R-free	0.27170
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.002
RMSD bond angle	0.491
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((dev_2650: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	3.400
Number of reflections	20683
<I/σ(I)>	3.9
Completeness [%]	93.4
Redundancy	2.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	0.2 M Tri-Sodium Citrate, 20 % PEG 3350