5V1H
DNA polymerase beta binary complex with 8-oxoG:A at the primer terminus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-11-28 |
Detector | DECTRIS PILATUS 200K |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 54.380, 79.240, 54.880 |
Unit cell angles | 90.00, 105.49, 90.00 |
Refinement procedure
Resolution | 39.620 - 1.946 |
R-factor | 0.2246 |
Rwork | 0.219 |
R-free | 0.27240 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3isb |
RMSD bond length | 0.007 |
RMSD bond angle | 0.923 |
Data scaling software | HKL-3000 |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.946 |
Number of reflections | 61220 |
<I/σ(I)> | 14.6 |
Completeness [%] | 100.0 |
Redundancy | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 291 | 50 mM imidazole, 350 mM sodium acetate, 17% PEG3350 |