5URE

Wild type rat CYPOR bound with NADP+ - reduced form

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X26C
Synchrotron site	NSLS
Beamline	X26C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2011-11-03
Detector	DECTRIS PILATUS 300K
Wavelength(s)	1.1
Spacegroup name	P 21 21 21
Unit cell lengths	102.095, 114.980, 118.134
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.860 - 2.300
R-factor	0.199
Rwork	0.199
R-free	0.24900
RMSD bond length	0.006
RMSD bond angle	1.300
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	MOLREP
Refinement software	CNS (1.3)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.300
Number of reflections	61912
<I/σ(I)>	21
Completeness [%]	97.2
Redundancy	4.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	292	PEG 4000, Sodium Acetate, HEPES