5UKH

Structure of TelC from Streptococcus intermedius B196

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 5.0.2
Synchrotron site	ALS
Beamline	5.0.2
Temperature [K]	100
Detector technology	CCD
Collection date	2016-07-26
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.979
Spacegroup name	C 2 2 21
Unit cell lengths	127.383, 132.689, 58.258
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.200 - 1.980
R-factor	0.2228
Rwork	0.222
R-free	0.24510
Structure solution method	SAD
RMSD bond length	0.008
RMSD bond angle	0.884
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHENIX
Refinement software	PHENIX (1.11.1_2575)

Data quality characteristics

	Overall
Low resolution limit [Å]	49.200
High resolution limit [Å]	1.980
Number of reflections	34824
<I/σ(I)>	11.4
Completeness [%]	100.0
Redundancy	25.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	0.1 M Sodium Acetate pH 4.6, 0.1 M CaCl2, 30% PEG400