5UHI

Structure of RORgt bound to

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	80
Detector technology	PIXEL
Collection date	2012-01-11
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	1
Spacegroup name	C 2 2 21
Unit cell lengths	104.350, 104.323, 123.577
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	39.864 - 3.198
R-factor	0.2632
Rwork	0.257
R-free	0.31810
RMSD bond length	0.003
RMSD bond angle	0.911
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((1.10_2155: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	39.864
High resolution limit [Å]	3.198
Number of reflections	10961
<I/σ(I)>	12.98
Completeness [%]	95.7
Redundancy	5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		293	12% 8K PEG, 100mM HEPES pH7.5