Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.2.1 |
| Synchrotron site | ALS |
| Beamline | 8.2.1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2015-08-30 |
| Detector | MARMOSAIC 325 mm CCD |
| Wavelength(s) | 1 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 181.937, 223.071, 63.208 |
| Unit cell angles | 90.00, 105.31, 90.00 |
Refinement procedure
| Resolution | 41.148 - 3.348 |
| R-factor | 0.234 |
| Rwork | 0.233 |
| R-free | 0.25760 |
| Structure solution method | SAD |
| RMSD bond length | 0.004 |
| RMSD bond angle | 2.034 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 3.348 |
| Number of reflections | 17949 |
| <I/σ(I)> | 9.5 |
| Completeness [%] | 51.5 |
| Redundancy | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | EVAPORATION | 5.5 | 293 | 0.1 M sodium citrate pH 5.5 , 0.1 M NaCl, 12% (vol/vol) PEG4000 |
