5TWU
Structure of Maternal Embryonic Leucine Zipper Kinase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-11-11 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9792 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 65.126, 78.599, 79.110 |
Unit cell angles | 90.00, 110.60, 90.00 |
Refinement procedure
Resolution | 48.171 - 2.603 |
R-factor | 0.1672 |
Rwork | 0.161 |
R-free | 0.23460 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4bl1 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.156 |
Data reduction software | HKL |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.2_1309) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.690 |
High resolution limit [Å] | 2.600 | 5.600 | 2.600 |
Rmerge | 0.073 | 0.033 | 0.632 |
Total number of observations | 85366 | ||
Number of reflections | 22978 | ||
<I/σ(I)> | 15.2 | ||
Completeness [%] | 99.8 | 98.7 | 100 |
Redundancy | 3.7 | 3.5 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 4000 |