5TOE

Pim-1 kinase in complex with a 7-azaindole

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 21-ID-F
Synchrotron site	APS
Beamline	21-ID-F
Temperature [K]	100
Detector technology	CCD
Collection date	2008-08-11
Detector	MARMOSAIC 225 mm CCD
Wavelength(s)	0.979
Spacegroup name	P 65
Unit cell lengths	97.246, 97.246, 81.081
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	42.109 - 2.301
R-factor	0.1936
Rwork	0.189
R-free	0.23270
RMSD bond length	0.013
RMSD bond angle	1.311
Refinement software	PHENIX ((1.10_2155: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	42.109
High resolution limit [Å]	2.301
Number of reflections	18965
<I/σ(I)>	2.76
Completeness [%]	97.7
Redundancy	13

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		277	0.1M imidazole, 1M NaAcetate, 20% glycerol pH 6.5