5TKL
Crystal structure of FBP aldolase from Toxoplasma gondii, condensation intermediate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X29A |
Synchrotron site | NSLS |
Beamline | X29A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-07-31 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.075 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 109.621, 109.621, 54.958 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.129 - 1.751 |
R-factor | 0.1502 |
Rwork | 0.148 |
R-free | 0.17690 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.005 |
RMSD bond angle | 0.804 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.780 |
High resolution limit [Å] | 1.750 | 4.750 | 1.750 |
Rmerge | 0.064 | 0.033 | |
Rmeas | 0.066 | 0.034 | |
Rpim | 0.019 | 0.009 | 0.404 |
Total number of observations | 427202 | ||
Number of reflections | 34234 | ||
<I/σ(I)> | 13.8 | ||
Completeness [%] | 99.9 | 99.9 | 99.6 |
Redundancy | 12.5 | 13.3 | 7.2 |
CC(1/2) | 0.999 | 0.611 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 296 | 0.1M Sodium Acetate, 0.2M Lithium Sulfate, 3.5% PEG 8000, 10% PEG 1000 |