5SVY
MORC3 CW in complex with histone H3K4me1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-09-05 |
Detector | DECTRIS PILATUS3 R CdTe 300K |
Wavelength(s) | 1.00 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 30.990, 70.660, 26.470 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.330 - 1.050 |
R-factor | 0.1234 |
Rwork | 0.123 |
R-free | 0.14650 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.334 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 35.330 |
High resolution limit [Å] | 1.000 |
Number of reflections | 60514 |
<I/σ(I)> | 23.8 |
Completeness [%] | 96.4 |
Redundancy | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 2.5 M (NH4)2SO4, 0.1 M sodium acetate |