5SGA

Structures of product and inhibitor complexes of Streptomyces griseus protease a at 1.8 Angstroms resolution. a model for serine protease catalysis

Experimental procedure

Spacegroup name	P 42
Unit cell lengths	55.160, 55.160, 54.780
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 1.800
R-factor	0.116
RMSD bond length	0.019
RMSD bond angle	0.036
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	1.800 *
Rmerge	0.085 *
Total number of observations	16136 *
Number of reflections	15254 *
Completeness [%]	80.7 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	equilibrium dialysis *	4.1 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	1 (%(w/v))
2	1	drop		1.3 (M)