5OCX
Crystal structure of ACPA E4 in complex with CII-C-13-CIT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-01-28 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9795 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 38.716, 99.602, 51.877 |
Unit cell angles | 90.00, 101.88, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.230 | 1.780 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.083 | 0.584 |
Rpim | 0.076 | 0.539 |
Number of reflections | 37660 | 1896 |
<I/σ(I)> | 7.5 | 1.3 |
Completeness [%] | 97.3 | 90 |
Redundancy | 3.1 | 2.7 |
CC(1/2) | 0.994 | 0.606 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 20% (w/v) PEG3350, 0.2 M ammonium citrate dibasic |