5OBX
Mycoplasma genitalium DnaK-NBD
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-10-03 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | H 3 |
Unit cell lengths | 157.921, 157.921, 64.697 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.000 - 1.780 |
R-factor | 0.18275 |
Rwork | 0.182 |
R-free | 0.20369 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5obw |
RMSD bond length | 0.010 |
RMSD bond angle | 1.484 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0189) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 78.960 | 1.830 |
High resolution limit [Å] | 1.780 | 1.780 |
Rmerge | 0.030 | 0.510 |
Rpim | 0.020 | 0.360 |
Number of reflections | 57432 | 8302 |
<I/σ(I)> | 16 | 1.7 |
Completeness [%] | 99.4 | 98 |
Redundancy | 4.8 | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | Tris-HCl, ammonium sulfate, potassium thiocyanate |