5NUB
Structure of human amniotic fluid RBP4 saturated with laurate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-02-18 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.0 |
Spacegroup name | H 3 |
Unit cell lengths | 102.610, 102.610, 73.134 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 1.600 |
R-factor | 0.1752 |
Rwork | 0.174 |
R-free | 0.20495 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 5nu6 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.678 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.470 | 1.690 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.054 | 0.481 |
Number of reflections | 37622 | |
<I/σ(I)> | 12.8 | 2.6 |
Completeness [%] | 99.3 | 98.7 |
Redundancy | 4.6 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 4.3 M NaCl, 100 mM Hepes, pH 7.5 |