5MWE
Complex between the Leucine Zipper (LZ, residues 490-567) and Centrosomin-motif 2 (CM2) domains of Drosophila melanogaster Centrosomin (Cnn)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-09-10 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9763 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 195.990, 36.500, 43.780 |
Unit cell angles | 90.00, 102.84, 90.00 |
Refinement procedure
Resolution | 36.099 - 2.020 |
R-factor | 0.2296 |
Rwork | 0.228 |
R-free | 0.26890 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 0.568 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.100 | 2.070 |
High resolution limit [Å] | 2.020 | 2.020 |
Rmerge | 0.031 | 0.616 |
Rpim | 0.020 | 0.398 |
Number of reflections | 19929 | 1450 |
<I/σ(I)> | 18.2 | 2.1 |
Completeness [%] | 98.8 | 98.7 |
Redundancy | 3.3 | 3.3 |
CC(1/2) | 0.999 | 0.677 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 294 | 20% (w/v) PEG 3350, 0.2M potassium/sodium tartrate |