5MOB
ABA RECEPTOR FROM TOMATO, SlPYL1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-04-25 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 0.93 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 87.470, 87.470, 55.751 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 28.631 - 1.669 |
| R-factor | 0.193 |
| Rwork | 0.191 |
| R-free | 0.22180 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.001 |
| Data scaling software | Aimless (v7.0) |
| Phasing software | MOLREP (v7.0) |
| Refinement software | PHENIX (1.7.2_869) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 28.630 | 1.700 |
| High resolution limit [Å] | 1.670 | 1.670 |
| Number of reflections | 27365 | |
| <I/σ(I)> | 17.1 | |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 6.1 | 6.1 |
| CC(1/2) | 0.990 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | MICROBATCH | 7 | 295 | 3.5 M de sulfato de amonio pH 7.0 |
