5MMQ

ABA RECEPTOR FROM CITRUS, CSPYL1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALBA BEAMLINE XALOC
Synchrotron site	ALBA
Beamline	XALOC
Temperature [K]	100
Detector technology	PIXEL
Collection date	2014-01-10
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.98
Spacegroup name	P 21 21 21
Unit cell lengths	63.064, 68.899, 107.438
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.519 - 1.800
R-factor	0.1815
Rwork	0.180
R-free	0.21320
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.841
Data scaling software	SCALA (v7.0)
Phasing software	MOLREP (v7.0)
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.790
High resolution limit [Å]	1.700	1.700
Number of reflections	99432
<I/σ(I)>	10.5	0.87
Completeness [%]	99.9	98
Redundancy	6.8	6.6
CC(1/2)	0.990

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	MICROBATCH	8.5	289.15	0.1M Tris pH 8.5, 0.2M MgCl2, 25% PEG 6K