Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-01-01 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 1.00002 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 56.960, 56.740, 100.070 |
| Unit cell angles | 90.00, 99.73, 90.00 |
Refinement procedure
| Resolution | 40.610 - 1.740 |
| Rwork | 0.165 |
| R-free | 0.19800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3duh |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.8.3_1479) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 41.000 | 1.850 |
| High resolution limit [Å] | 1.740 | 1.740 |
| Rmeas | 0.054 | 0.636 |
| Number of reflections | 63104 | |
| <I/σ(I)> | 13.7 | 1.8 |
| Completeness [%] | 97.9 | 91.1 |
| Redundancy | 3.4 | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 294 | 20.75% PEG 3350, 200MM SODIUM SULPHATE |
