5M9V
Human angiogenin PD/ALS variant R121C
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-05-29 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.9200 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 82.539, 118.969, 37.409 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 67.800 - 1.700 |
R-factor | 0.21025 |
Rwork | 0.209 |
R-free | 0.23883 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ang |
RMSD bond length | 0.011 |
RMSD bond angle | 1.374 |
Data reduction software | DIALS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0151) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 67.800 | 1.730 |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 20751 | |
<I/σ(I)> | 7.3 | 0.9 |
Completeness [%] | 99.7 | 98.6 |
Redundancy | 5.1 | 5.1 |
CC(1/2) | 0.997 | 0.470 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 289 | 0.2 M Na/K tartrate 0.1 M bis-tris propane 16% PEG 4000 |