5LYE
Re-refined structure of the bacteriophage T4 short tail fibre PDB entry 1H6W containing 71 additionally identified residues
Replaces: 1H6WExperimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2000-06-01 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.933 |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 51.257, 51.257, 249.491 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.800 - 1.900 |
R-factor | 0.18473 |
Rwork | 0.183 |
R-free | 0.21465 |
Structure solution method | SIRAS |
RMSD bond length | 0.017 |
RMSD bond angle | 1.603 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SOLVE |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.800 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.057 | 0.154 |
Number of reflections | 28682 | |
<I/σ(I)> | 8.5 | 4.8 |
Completeness [%] | 92.3 | 68.7 |
Redundancy | 7.3 | 5.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 293 | 15-25 % (V/V) 2-METHYLPROPANE-2-OL (TERTIARY BUTANOL), 100 MM SODIUM CITRATE PH 5.6 10% (V/V) GLYCEROL, 10 MM HEPES, 150 MM SODIUM CHLORIDE |