5LOX
Helical Assembly of the Anbu Complex from Pseudomonas aeruginosa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-12-13 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 150.070, 230.080, 171.720 |
Unit cell angles | 90.00, 108.39, 90.00 |
Refinement procedure
Resolution | 39.600 - 2.900 |
R-factor | 0.19886 |
Rwork | 0.198 |
R-free | 0.21840 |
Structure solution method | SAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.446 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | SHELXDE |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.600 | 3.070 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.172 | 1.193 |
Number of reflections | 244138 | |
<I/σ(I)> | 14.33 | 2.31 |
Completeness [%] | 99.6 | 98.2 |
Redundancy | 14.2 | 14.1 |
CC(1/2) | 0.998 | 0.822 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 295 | 0.1 M sodium acetate pH 4.8, 1.2 M sodium nitrate |